响应曲面优化粗锡真空蒸馏

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蒲正浩^1,2,3，韩继标^1,2,3，李一夫^1,2*，杨斌^1,2,3，戴永年^1,2

1. 昆明理工大学真空冶金国家工程实验室，云南昆明 650093；2. 复杂有色金属资源清洁利用国家重点实验室，云南昆明 650093; 3. 云南省有色金属真空冶金重点实验室，云南昆明 650093

收稿日期:2017-08-14修回日期:2017-10-20出版日期:2018-06-22发布日期:2018-06-06
通讯作者:李一夫

基金资助:As-Pb混合蒸汽冷凝机理的研究

Optimization of Crude Tin Vacuum Distillation by Response Surface Methodology

Zhenghao PU^1,2,3, Jibiao HAN^1,2,3, Yifu LI^1,2*, Bin YANG^1,2,3, Yongnian DAI^1,2

1. National Engineering Lab for Vacuum Metallurgy, Kunming University of Science and Technology, Kunming, Yunnan 650093, China; 2. State Key Laboratory of Complex Non-ferrous Metal Resources Clear Utilization, Kunming, Yunnan 650093, China; 3. Key Laboratory of Vacuum Metallurgy for Nonferrous Metal of Yunnan Province, Kunming, Yunnan 650093, China

Received:2017-08-14Revised:2017-10-20Online:2018-06-22Published:2018-06-06
Contact:LI Yi-fu

摘要/Abstract

摘要： 采用响应曲面法优化粗锡真空蒸馏工艺，研究了蒸馏温度、保温时间和原料质量对粗锡真空蒸馏提纯效果的影响. 结果表明，蒸馏温度和保温时间对粗锡真空蒸馏影响较大，原料质量的影响较小，蒸馏温度1350~1400℃、保温时间40~60 min时可有效去除粗锡中杂质. 以97.4185%的粗锡为原料，在蒸馏温度1400℃、保温60 min的条件下，锡纯度达99.8752%，含0.012% Pb, 0.045% Sb, 0.0005% Bi和0.0005% As，Fe和Cu含量无变化，Sn直收率达99.89%.

引用本文

蒲正浩韩继标李一夫杨斌戴永年. 响应曲面优化粗锡真空蒸馏[J]. 过程工程学报, 2018, 18(3): 496-502.
Zhenghao PU Jibiao HAN Yifu LI Bin YANG Yongnian DAI. Optimization of Crude Tin Vacuum Distillation by Response Surface Methodology[J]. Chin. J. Process Eng., 2018, 18(3): 496-502.

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