摘要/Abstract

建立了一种以N-氟代双苯磺酰胺（NFSI）为氧化剂合成二硫化合物的新方法.该方法反应温和、操作简便、反应时间短并无过度氧化的副产物（亚砜或砜类化合物）生成.
关键词: N-氟代双苯磺酰胺, 氧化, 二硫化合物
A simple and rapid method is developed for the oxidation of thiols to the corresponding disulfides using N-fluorobenzenesulfonimide (NFSI) as the oxidant without any contamination by over oxidation. The synthetic protocol for disulfide bond formation proceeded efficiently under external base-and metal-free conditions with the advantages of simple operation, mild reaction conditions as well as short reaction times.
Key words: N-fluorobenzenesulfonimide, oxidation, disulfide


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