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Study of Thermal Radiation Properties of Pyrolytic Carbon Protective Coatings for Monocrystalline Si

本站小编 哈尔滨工业大学/2019-10-24

Study of Thermal Radiation Properties of Pyrolytic Carbon Protective Coatings for Monocrystalline Silicon Furnace

Wei-Wei Cao1,2, Bo Zhu3, Wei Zhao3, Yong-Wei Wang3, Yang Chen3, Xi-Hai Wang4

(1.College of Materials Science and Engineering, Tianjin Polytechnic University, Tianjin 300387, China; 2.Taishan Sports Industry Group, Leling 253600, China; 3.College of Materials Science and Engineering, Shandong University, Ji’nan 250061, China; 4. Weifang Wuzhou Wind Power Equipment Co., Ltd, Weifang 262100, China)



Abstract:

The thermal radiation properties of pyrolytic carbon (PyC) protective coatings for monocrystalline silicon furnace prepared by different processes were tested. The changes of normal emissivity of carbon materials caused by PyC protective coatings were discussed, and the influence of phase structure and surface appearance on the thermal radiation properties was investigated. The results show that the thermal radiation properties of PyC protective coatings with the wave band of 5-25 μm are better than C/C substrate, further, normal spectral emissivity of CVD PyC coating remains basically at 0.85-0.90, and the normal total emissivity can reach 0.89, which shows high thermal radiation performance. For resin PyC coating and CVD PyC coating, the degree of graphitization are 44.53% and 16.28% respectively, and the R value of Raman spectrum are 0.964 and 1.384 respectively. Relatively disorder graphite structure of the latter causes various vibration modes, and the spectral emissivity is better, so the thermal radiation property of CVD PyC coating is excellent. A lot of spherical particles exists on the surface of the CVD PyC coating, and the more interface and spacing of particles reduce the number of particles per unit volume. Therefore, the scattering of thermal radiation is strongly strengthened, and the spectral emissivity is higher.

Key words:  Monocrystalline silicon furnace  PyC protective coating  Normal spectral emissivity  Normal total emissivity  Graphite structure

DOI:10.11916/j.issn.1005-9113.2013.04.007

Clc Number:TB332

Fund:


相关话题/Study Thermal Radiation Properties Pyrolytic